HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 13388361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | HCID 53957614 | HCID 53957614 | — |
| Product | HCID 13388361 | HCID 13388361 | 96% |
Reaction Steps
0.9 g (0.01 mol) of aniline was reacted with 1.8 g (0.01 mol) of 3,4-dimethyl-3-cyclohexene dicarboxylic anhydride under reflux for 4 hours in isopropyl ether. The reaction mixture was cooled, and the precipitated crystals were filtered off to provide 2.6 g (yield: 96%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04596826 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-e3d9294c53334d6f8123e877881f6bd7 |
| Source note | uspto-grants-1986_06 |