Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-Butylmethacrylamide | HCID 9855497 | — |
Reaction Steps
In a 1 liter 3-necked flask were combined 400 ml dry THF and 40 ml distilled n-butylamine (0.405 mol). After cooling to 5° C. in an ice bath, 20 ml (0.205 mol) methacryloyl chloride was added slowly so as to keep the temperature below 10° C. The precipitate was removed by filtration, and the filtrate concentrated on a rotary evaporator. 1 g DNPD was added and the oil distilled at 76°-78° C. and 20 m torr. Yield 24.3 g (84%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04596858 |
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| Source dataset | uspto-grants-1986_06 |
|---|
| ORD ID | ord-ed2f99d572ba441ea7927338c4b4af02 |
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| Source note | uspto-grants-1986_06 |
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