HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1982527Generated: November 3, 2026
Potassium Carbonate → HCID 13633265, compound
https://huagongshe.com/reaction/1982527
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Chloro-3-nitrophenyl cyclopropyl ketone | HCID 1268259 | — |
| Reactant | Acetic Acid Mixture with Hydrobromic Acid | HCID 21893785 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 13633265 | HCID 13633265 | — |
Reaction Steps
20 g (88.6 mmol) of 4-chloro-3-nitrophenyl cyclopropyl ketone is added to a solution of 65 m of 32% HBr/acetic acid in 300 ml acetic acid and heated to 80° C. for 5 hr. The reaction mixture is cooled to room temperature and poured nto 1 L of 10% potassium carbonate solution, dried over MgSO4 filtered and treated with charcoal. The solvent is removed in vacuo, and the residue is crystallized from ether to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04596872 |
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| Source dataset | uspto-grants-1986_06 |
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| ORD ID | ord-a4f60d8f66334188b2393a08d693cf29 |
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| Source note | uspto-grants-1986_06 |
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