HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 13764015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | p-Anisoylcyclopropane | HCID 81580 | — |
| Product | HCID 13764015 | HCID 13764015 | — |
Reaction Steps
Combine 25 g (0.14 mol) of cyclopropyl 4-methoxyphenyl ketone with 50 g (0.73 mol) of imidazole, and heat to 200°-225° C. for 24 hr. Isolation from 200 g of silica gel using 2% methanol/methylene chloride followed by crystallization from methanol provides the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04596872 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-3dfc67400a2e4afe9c9c70d86d0df603 |
| Source note | uspto-grants-1986_06 |