HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 23316950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | HCID 571501 | HCID 571501 | — |
| Product | HCID 23316950 | HCID 23316950 | — |
Reaction Steps
Combine 15 g (0.10 mol) of cyclopropyl 4-pyridinyl ketone with 30 g (0.44 mol) of imidazole and heat to 180°-200° C. for 24 hr. Isolation from 200 g silica gel using 5% methanol/methylene chloride followed by crystallization from ether provides the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04596872 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-efedabfea9194b4a83903557a53ef1e6 |
| Source note | uspto-grants-1986_06 |