HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 13764019, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | 3-(4-Fluorobenzoyl)propyl chloride | HCID 19750 | — |
| Product | HCID 13764019 | HCID 13764019 | — |
Reaction Steps
Combine 50 g (0.25 mol) of 4-chloro-4'-fluorobutyrophenone with 120 g (1.76 mol) of imidazole, and heat to 175° C. for 18 hr. Isolation of the product from 500 g of silica gel, followed by crystallization from ethyl acetate, provides the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04596872 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-0476a2a9ebaa4b969d12233b1202efb6 |
| Source note | uspto-grants-1986_06 |