HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 13764021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | 4-Chloro-4'-methylbutyrophenone | HCID 98745 | — |
| Product | HCID 13764021 | HCID 13764021 | — |
Reaction Steps
Combine 100 g (0.51 mole) of 4-chloro-4'-methylbutyrophenone with 300 g (4.4 mole) of imidazole and heat to 175° C. under nitrogen for 24 hr. Purification from 1 kg of silica gel using methylene chloride as solvent, followed by crystallization from ether provides the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04596872 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-6c0940217bbf4edeb083c55acd23ef30 |
| Source note | uspto-grants-1986_06 |