HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Benzyloxybenzyl)benzyl alcohol → 4-(2-Benzyloxybenzyl)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Benzyloxybenzyl)benzyl alcohol | HCID 68872241 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-(2-Benzyloxybenzyl)benzaldehyde | HCID 21909304 | 97.6% |
Reaction Steps
To a solution of 4-(2-benzyloxybenzyl)benzyl alcohol (1.0 g) in dichloromethane (50 mL) was added manganese dioxide (10 g), and the mixture was stirred at room temperature for 3 hours. After insoluble materials were removed by filtration, the solvent of the filtrate was removed under reduced pressure to give 4-(2-benzyloxybenzyl)benzaldehyde (0.97 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07541341B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-d6fec15306f945098762beb3c9d76b43 |
| Source note | uspto-grants-2009_06 |