4-Chlorobenzyl alcohol → HCID 67528502, compound

HRID 1982895Notes

Reaction equation

HRID 1982895 reaction equation
Br[C:2]1[CH:3]=[N+:4]([O-])[CH:5]=[CH:6][C:7]=1[N+:8]([O-:10])=[O:9].[Cl:12][C:13]1[CH:20]=[CH:19][C:16]([CH2:17][OH:18])=[CH:15][CH:14]=1>>[Cl:12][C:13]1[CH:20]=[CH:19][C:16]([CH2:17][O:18][C:2]2[CH:3]=[N:4][CH:5]=[CH:6][C:7]=2[N+:8]([O-:10])=[O:9])=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 133974-Chlorobenzyl alcoholHCID 5485213-Bromo-4-nitropyridine N-oxide

Product 1

HCID 67528502HCID 67528502, compoundYield 25.3%

Procedure

In accordance with the same procedures as in Steps 3 and 4 of Preparation 1, except for using 3-bromo-4-nitropyridin-N-oxide prepared in Step 2 of Preparation 1 and 4-chlorobenzyl alcohol, the titled compound was obtained as a white solid. (Yield: 25.3% )

Workup

  1. customIn accordance with the same procedures as in Steps 3 and 4 of Preparation 1

Sources & evidence

ORD record
ord-86b5a30fd46c45a98d878ac6ee20d232
Source dataset
uspto-grants-2009_06
Patent number
US07541366B2

Reaction notes

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