HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 23149186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 23149160 | HCID 23149160 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23149186 | HCID 23149186 | — |
Reaction Steps
1.21 g of 1-(hydroxymethyl)-3-formyl-1H-pyrazole was dissolved to 50 ml of dichloromethane. 2.4 ml of thionyl chloride was added to the solution, followed by stirring at room temperature for overnight. The reaction mixture was concentrated under reduced pressure to obtain 1.57 g of 1-(chloromethyl)-3-formyl-1H-pyrazole hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07541374B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-47484155c0a14f7485e51d78cdfcb41e |
| Source note | uspto-grants-2009_06 |