Acetone → HCID 23149150, compound

Participants

Reaction Conditions

Reaction Steps

The mixture of 1.15 g of 3-i-propyl-1H-1,2,4-triazole, 0.94 g of paraformaldehyde and 0.14 g of triethylamine was stirred at 150° C. for 5 hours. After the reaction mixture was cooled to room temperature, acetone was added. The mixture was filtered. The filtrate was concentrated under reduced pressure. Hexane was added to the obtained residue, as a result, a crystal was formed. The crystal was collected to obtain 1.28 g of 3-i-propyl-1H-triazole-1-ylmethanol.

Provenance & Evidence