Thionyl Chloride → HCID 23149161, compound

Participants

Reaction Steps

1.28 g of 3-i-propyl-1H-1,2,4-triazole1-ylmethanol was dissolved to 20 ml of dichloromethane, and 2 ml of thionyl chloride was added to the solution, followed by stirring at room temperature for 8 hours. The reaction mixture was concentrated under reduced pressure. Diethylether was added to the residue, as a result, a crystal was formed. The crystal was collected to obtain 1.58 g of 1-(chloromethyl)-3-i-propyl-1H-1,2,4-triazole hydrochloride.

Provenance & Evidence