참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Formaldehyde | HCID 712 | — |
| 반응물 | 3-(pentafluoroethyl)-1H-pyrazole | HCID 178506326 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 3-(pentafluoroethyl)-1H-pyrazole-1-ylmethanol | HCID 23149136 | 91.7% |
반응 단계
The mixture of 1.86 g of 3-(pentafluoroethyl)-1H-pyrazole and 0.60 g of paraformaldehyde was stirred at 130° C. for 5 hours. After the reaction mixture was cooled to room temperature, acetone was added. The mixture was filtered. The filtrate was concentrated under reduced pressure to obtain 1.98 g of 3-(pentafluoroethyl)-1H-pyrazole-1-ylmethanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07541374B2 |
|---|
| 출처 데이터셋 | uspto-grants-2009_06 |
|---|
| ORD ID | ord-43c92962c4fa4633a2ee2347d7f766f7 |
|---|
| 출처 메모 | uspto-grants-2009_06 |
|---|
