HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 860807-68-7
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 23149206 | HCID 23149206 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 860807-68-7 | HCID 23149144 | — |
Reaction Steps
1.69 g of 3-cyano-1H-indole-1-ylmethanol was dissolved to 30 ml of dichloromethane. 1.4 ml of thionyl chloride was added to the solution, followed by stirring at room temperature for 3 hours. The reaction mixture was concentrated under reduced pressure to obtain 1.70 g of 1-(chloromethyl)-3-cyano-1H-indole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07541374B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-560711731de94df7b3ec5ecf1e48f2dd |
| Source note | uspto-grants-2009_06 |