HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 23149146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 23149182 | HCID 23149182 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 23149146 | HCID 23149146 | — |
Reaction Steps
0.22 g of 4-{[dichlorofluoromethyl]thio}-1H-pyrazole-1-ylmethanol was dissolved to 10 ml of chloroform. 0.3 ml of thionyl chloride was added to the solution, and refluxed for 4 hours. The reaction mixture was concentrated under reduced pressure to obtain 0.21 g of 1-(chloromethyl)-4-{[dichloro(fluoro)methyl]thio}-1H-pyrazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07541374B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-6b2fd82e842a4c069fd14c3887b6affe |
| Source note | uspto-grants-2009_06 |