HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiomorpholine → HCID 67215239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiomorpholine | HCID 67164 | — |
| Reactant | HCID 86613584 | HCID 86613584 | — |
| Product | HCID 67215239 | HCID 67215239 | 59% |
Reaction Steps
As described for example 136b, 2-chloro-5-[5-(5-methyl-3-phenyl-isoxazol-4-yl)-[1,3,4]oxadiazol-2-yl]-pyridine (400 mg, 1.18 mmol) was converted using thiomorpholine instead of morpholine to the title compound (126 mg, 59%) which was obtained as an off-white solid. MS: m/e=406.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07541372B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-4d2a9fdf7dc14c9185291307c94d41b6 |
| Source note | uspto-grants-2009_06 |