HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68845319, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 131727458 | HCID 131727458 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68845319 | HCID 68845319 | — |
Reaction Steps
The crude product from step 1 was dissolved in methylene chloride (6.4 mL) and treated with trifluoroacetic acid (3.6 mL). After stirring for 1.5 hours the reaction was concentrated and the residue was partitioned between methylene chloride and aqueous sodium bicarbonate solution. The organic layer was dried (sodium sulfate) and concentrated to afford a gray-green solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07541466B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-80d24c805bff4921a38add119608acce |
| Source note | uspto-grants-2009_06 |