HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 68844355, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 3-Bromo-4-methoxybenzonitrile | HCID 736049 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 68844355 | HCID 68844355 | — |
Reaction Steps
Phenol and 3-bromo-4-methoxybenzonitrile were subjected to Ullman ether coupling according to the procedure described in synthetic method 9 to afford product as a white solid: 1H NMR (CDCl3) δ 7.43 (dd, J=8.6, 2.0 Hz, 1H), 7.40-7.32 (m, 2H), 7.19-7.11 (m, 2H), 7.03 (d, J=8.6 Hz, 1H), 7.01-6.94 (m, 2H), 3.93 (s, 3H) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07541466B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-bb3893fbe558426686537b18957754b9 |
| Source note | uspto-grants-2009_06 |