HRID1983967

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=C1OC(=O)c2cc([N+](=O)[O-])cc3cccc1c23

HCID18194

Naphthalic anhydride, 3-nitro-

C12H5NO5

HCID68830082

未命名化合物

PRODUCTS

生成物

结构：COc1ccc(N2C(=O)c3cccc4cc([N+](=O)[O-])cc(c34)C2=O)c(NCCO)c1

HCID68828355

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

结构：CCN(CCO)c1ccc(N2C(=O)c3cccc4c([N+](=O)[O-])ccc(c34)C2=O)cc1

溶剂HCID86613406

未命名化合物

PROCEDURE

实验过程

The reaction of N-(2-hydroxyethyl)-5-methoxy-2-aminoaniline with 3-nitronaphthalene-1,8-dicarboxylic anhydride in imidazole (synthesis and work-up as in Example 2, Step 1) afforded the product as a dark-red powder. For purification, the crude product in ethanol/acetone was filtered through a bed of silica gel UV/Vis (CHCl3: λmax: 411, 524 nm