HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 57717900, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 68869428 | HCID 68869428 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57717900 | HCID 57717900 | 99.4% |
Reaction Steps
To a stirring solution of 0.4 g (1.05 mmol) of the above ester in 2.5 ml of THF, 0.6 ml of MeOH was added along with 0.6 ml of 2N LiOH at rt. Usual work up as described in general procedure C gave 0.38 g of title compound as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07544699B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-701c5455011240c3ad42ef083d3801ed |
| Source note | uspto-grants-2009_06 |