HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Aminoquinoline → 4-bromo-N-quinolin-7-ylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Aminoquinoline | HCID 11377 | — |
| Reactant | 4-Bromobenzoyl chloride | HCID 68515 | — |
| Product | 4-bromo-N-quinolin-7-ylbenzamide | HCID 831408 | — |
Reaction Steps
This material was prepared analogous to the procedure described for Example 1(c). 4-Bromo-benzoyl chloride (2.19 g, 10 mmol, Aldrich) reacted with 7-amino-quinoline (1.22 g, 8.5 mmol, prepared according to the procedure described in WO03099284) to give the title compound. MS (ESI, pos. ion) m/z: 328 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07544803B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-2ba21dbe15374c9dbfd51f2d89214263 |
| Source note | uspto-grants-2009_06 |