HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Formylphenylboronic acid → 2'-Formyl-biphenyl-4-carboxylic acid quinolin-7-ylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Formylphenylboronic acid | HCID 292189 | — |
| Reactant | 4-bromo-N-quinolin-7-ylbenzamide | HCID 831408 | — |
| Product | 2'-Formyl-biphenyl-4-carboxylic acid quinolin-7-ylamide | HCID 11187278 | — |
Reaction Steps
This material was prepared analogous to the procedure described for Example 1(a). 4-Bromo-N-quinolin-7-yl-benzamide, Example 27, (327 mg, 1 mmol) reacted with 2-formylphenyl boronic acid (183 mg, 1.1 mmol, Aldrich) to give the title compound as a yellow solid. Mp 258-260° C. MS (ESI, pos. ion) nz/z: 353 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07544803B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-c9c6ae45acfb4c5e8525ebfb5147f818 |
| Source note | uspto-grants-2009_06 |