HCID 10218034, compound → HCID 68867530, compound

Participants

Reaction Steps

2-(2-Allyl-4-{3-[1-(4-tert-butyl-benzyl)-3-methyl-2-oxo-imidazolidin-4-yl]-propyl}-phenoxy)-2-methyl-propionic acid methyl ester (0.060 g, 0.115 mmole) was dissolved in absolute ethanol (10 mL). After purged the solution with N2 for 15 min, 10% Pd/C (0.030 g). The reaction was stirred under a hydrogen balloon at room temperature for 2 hours. The catalyst was removed through filtration, and solvent was removed on rota-vapor to provide a colorless oil (0.053 g, 88%). Mass [EI+] 523 (M+H)+.

Provenance & Evidence