HCID 68869975, compound → HCID 68867342, compound

Participants

Reaction Steps

2-(4-{3-[1-(4-tert-Butyl-benzyl)-3-methyl-2-oxo-imidazolidin-4-yl]-propyl}-2-methyl-phenoxy)-2-methyl-propionic acid methyl ester (0.620 g, 1.25 mmole) was dissolved in 20% HOAc in EtOAC (50 mL). After purged the solution with N2 for 15 min, 10% Pd/C (0.600 g). The reaction was stirred under a hydrogen balloon at room temperature for overnight. The catalyst was removed through filtration, and solvent was removed on rota-vapor to provide a colorless oil (0.337 g, 77%). Mass [EI+] 349 (M+H)+.

Provenance & Evidence