HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → (1SR,8RS)-5-(2,2-Dimethyl-propyl)-6-methyl-3,4-diaza-tricyclo[6.2.1.02,7]undeca-2,4,6-triene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Bicyclo(2.2.1)heptane-2,3-dione | HCID 138696 | — |
| Reactant | (1,4,4-Trimethyl-2-oxo-pentyl)-phosphonic acid diethyl ester | HCID 86617458 | — |
| Product | (1SR,8RS)-5-(2,2-Dimethyl-propyl)-6-methyl-3,4-diaza-tricyclo[6.2.1.02,7]undeca-2,4,6-triene | HCID 69059729 | — |
Reaction Steps
light-yellow oil. MS (ESI): 297.1 (MH+). Prepared from bicyclo[2.2.1]heptane-2,3-dione, (1,4,4-trimethyl-2-oxo-pentyl)-phosphonic acid diethyl ester, hydrazine monohydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07547697B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-176fec6a1ae14e0cb5e5b253028b237f |
| Source note | uspto-grants-2009_06 |