HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → (1SR,8RS)-5-tert-Butyl-3,4-diaza-tricyclo[6.2.1.02,7]undeca-2,4,6-triene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Bicyclo(2.2.1)heptane-2,3-dione | HCID 138696 | — |
| Reactant | Dimethyl (3,3-dimethyl-2-oxobutyl)phosphonate | HCID 14302170 | — |
| Product | (1SR,8RS)-5-tert-Butyl-3,4-diaza-tricyclo[6.2.1.02,7]undeca-2,4,6-triene | HCID 69058595 | — |
Reaction Steps
off-white crystalline solid. MS (EI): 245.2 (M+). Prepared from bicyclo[2.2.1]heptane-2,3-dione, (3,3-dimethyl-2-oxo-butyl)-phosphonic acid dimethyl ester, hydrazine monohydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07547697B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-084567cbae85410e9f4a1985da07c180 |
| Source note | uspto-grants-2009_06 |