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HRID1985619

反应详情

EQUATION

反应方程式

HRID 1985619 的结构方程式

REACTANTS

反应物

3
结构：NN.O
HCID24654

Hydrazine hydrate (1:1)

H6N2O

结构：CC1(C)[C@@H]2CC[C@@]1(C)C(=O)C2=O
HCID641916

未命名化合物

结构：COP(=O)(CC(=O)C(C)(C)C)OC
HCID14302170

Dimethyl (3,3-dimethyl-2-oxobutyl)phosphonate

C8H17O4P

PRODUCTS

生成物

1
结构：CC(C)(C)c1cc2c(nn1)[C@]1(C)CC[C@H]2C1(C)C
HCID69061134

未命名化合物

PROCEDURE

实验过程

light yellow oil. MS (ESI): 245.2 (MH+). Prepared from (1R,4S)-1,7,7-trimethyl-bicyclo[2.2.1]heptane-2,3-dione, (3,3-dimethyl-2-oxo-butyl)-phosphonic acid dimethyl ester, hydrazine monohydrate. Main product isolated and purified by silica gel chromatography.

WORKUP

后处理

  1. customMain product isolated
  2. custompurified by silica gel chromatography