HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Triphenylmethyl)pyridinium tetrafluoroborate → HCID 69063830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Triphenylmethyl)pyridinium tetrafluoroborate | HCID 9909412 | — |
| Reactant | HCID 86608947 | HCID 86608947 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69063830 | HCID 69063830 | 98.4% |
Reaction Steps
To a solution of 0.25 g of the product of step 1 in 5 ml dichloromethane was added 0.25 g tritylpyridinium tetrafluoroborate at room temperature and the mixture was stirred at this temperature for 2 h. The reaction mixture was purified by chromatography on silica gel with dichlorometha:ethyl aceate=19:1 to yield 0.39 g of the title compound as colorless foam (MS: 656.3 and 658,4 (M+H+)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07547699B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-33f84ec3f730424ea2ae1f6ccd9b8071 |
| Source note | uspto-grants-2009_06 |