HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69036038, compound → HCID 69037775, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69036038 | HCID 69036038 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69037775 | HCID 69037775 | — |
Reaction Steps
To a solution of 5 g (16.06 mmol) of 4-tert-butoxycarbonylamino-4-cyanomethyl-piperidine-1-carboxylic acid ethyl ester in 107 ml of methanol was added 4.71 g of Raney Nickel catalyst. The suspension was hydrogenated under 55 psi pressure at room temperature during 3 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07547705B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-4b246b9dccfb49018b089dabb998b34b |
| Source note | uspto-grants-2009_06 |