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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1985846Generated: November 2, 2026

HCID 57720285, compound → HCID 57720276, compound

https://huagongshe.com/reaction/1985846

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57720285HCID 57720285—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 57720276HCID 57720276100.3%

Reaction Conditions

Temperature60 °C

Reaction Steps

2-[3-(4-Benzyloxybutyloxy)benzylamino]-1-(β-D-ribofuranosyl)-1H-benzimidazole (24 mg) was dissolved in ethanol (2 mL). To the solution was added a catalytic amount of 10% palladium-carbon powder, and the mixture was stirred at 60° C. under a hydrogen atmosphere for 24 hour. The insoluble material was removed by filtration, and the solvent of the filtrate was removed under reduced pressure to give the title compound (20 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07547680B2
Source datasetuspto-grants-2009_06
ORD IDord-4ff368cf81f24504b38875f20592fca7
Source noteuspto-grants-2009_06