HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexamethylenetetramine → 3,5-Difluoro-4-hydroxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexamethylenetetramine | HCID 4101 | — |
| Reactant | 2,6-Difluorophenol | HCID 94392 | — |
| Reactant | Acetic acid--water (1/1) | HCID 21899381 | — |
| Product | 3,5-Difluoro-4-hydroxybenzaldehyde | HCID 10192584 | — |
Reaction Steps
2,6-difluorophenol (1 eq) and hexamethylenetetramine (2 eq) were dissolved in a water/acetic acid mixture (10:90). The reaction mixture was refluxed for 18 hours then cooled to room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07547729B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-b18ec6546f094b1da3c4822f3ddb8a6f |
| Source note | uspto-grants-2009_06 |