HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86625367, compound → HCID 68856069, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86625367 | HCID 86625367 | — |
| Solvent | HCID 68856920 | HCID 68856920 | — |
| Product | HCID 68856069 | HCID 68856069 | — |
Reaction Steps
Using the method of Preparation C in 2-{5-chloro-2-[3-(4-methylpiperazin-1-yl)-propylamino]-pyrimidin-4-yl}-benzo[b]thiophene-4-carboxylic acid amide tri-hydrochloride, the title compound is synthesized from 2-{5-chloro-2-[3-(4-methyl-piperazin-1-yl)-propylamino]-pyrimidin-4-yl}-benzo[b]thiophene-6-carboxylic acid [bis-(4-methoxyphenyl)-methyl]-amide and isolated as a yellow solid. ES+(m/z) 445 (35Cl) and 447 (37Cl) [M+H].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07547691B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-57e1394e13b44b41ba0aa94a39fe0bcb |
| Source note | uspto-grants-2009_06 |