HRID1986236

反应详情

EQUATION

反应方程式

HRID 1986236 的结构方程式

PROCEDURE

实验过程

Using the method of 2-[5-chloro-2-(3-piperazin-1-ylpropylamino)-pyrimidin-4-yl]-benzo[b]thiophene-4-carboxylic acid cyclopropylamide tri-hydrochloride, the title compound is synthesized from [2-(2,5-dichloropyrimidin-4-yl)-benzo[b]thiophen-6-yl]-morpholin-4-yl-methanone and 4-(3-aminopropyl)-piperazine-1-carboxylic acid tert-butyl ester and isolated as a yellow solid. ES+(m/z) 501 (35Cl) and 503 (37Cl) [M+H].

WORKUP

后处理

  1. customisolated as a yellow solid