HRID1986241

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID78328

1-Piperazinepropanamine, 4-methyl-

C8H19N3

结构：CN1CCN(CCCNc2nccc(-c3cc4ccccc4s3)n2)CC1.Cl.Cl.Cl

HCID68855962

未命名化合物

HCID86625370

未命名化合物

PRODUCTS

生成物

结构：COc1cccc2cc(-c3nc(NCCCN4CCN(C)CC4)ncc3Br)sc12.Cl.Cl.Cl

HCID68856938

未命名化合物

PROCEDURE

实验过程

Using the method of [4-(benzo[b]thiophen-2-yl)-pyrimidin-2-yl]-[3-(4-methylpiperazin-1-yl)-propyl]-amine tri-hydrochloride, the title compound is prepared from 5-bromo-2-chloro-4-(7-methoxy-benzo[b]thiophen-2-yl)-pyrimidine and 1-(3-aminopropyl)-4-methylpiperazine and isolated as a yellow solid. ES+(m/z) 476 (79Br) and 478 (81Cl) [M+H].

WORKUP

后处理

customisolated as a yellow solid