HCID 68871620, compound → HCID 68869859, compound

Participants

Reaction Steps

To a solution of the product of Step 2 in MeOH (180 mL) and EtOAC (50 mL), was added 10% palladium on carbon (280 mg). This mixture was then stirred under hydrogen atmosphere for 36 h. The reaction mixture was filtered and then concentrated to afford the title compound, which was used directly to next step without further purification. MS (ES+) m/e 260 [M+H]+.

Provenance & Evidence