HRID1986540

反应详情

EQUATION

反应方程式

HRID 1986540 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

230 mg of 33 (1.235 mmol) are taken up in a 25 ml round-bottomed flask and 5 ml of a solution of hydrogen chloride in dioxane (4M) are added. The medium is stirred for 2 hours at room temperature under argon. After evaporating off the solvent, 230 mg of amine 34 are obtained in hydrochloride form, which product is used directly in the following step.

WORKUP

后处理

  1. customAfter evaporating off the solvent, 230 mg of amine 34
  2. customare obtained in hydrochloride form, which product