HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethylpiperazine, trans- → HCID 136360191, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethylpiperazine, trans- | HCID 220672 | — |
| Reactant | 8-chloro-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 3653116 | — |
| Product | HCID 136360191 | HCID 136360191 | 5.6% |
Reaction Steps
8-Chloro-5,10-dihydro-dibenzo[b,e][1,4]diazepine-11-one (25 mg, 0.1 mmol) and trans-2,5-dimethylpiperazine (114 mg, 1.0 mmol) were reacted according to GP4 to give 1.9 mg of the title compound (160FE33A). MS (ESI) 341 (MH+). Purity for MH+ (UV/MS) 100/82.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07550454B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-3017542d66994bad9c8bc16bbc7f18c3 |
| Source note | uspto-grants-2009_06 |