Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 68867784 | HCID 68867784 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 68869071 | HCID 68869071 | — |
Reaction Steps
10 g of intermediate A1 and 200 ml of an aqueous solution of NH3 (32%) are mixed in an autoclave and heated up to 130° C. for 8 hours. The reaction mixture is diluted with 200 ml water. The precipitated reaction product is separated washed with water and dichloro methane and dried at reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07550465B2 |
|---|
| Source dataset | uspto-grants-2009_06 |
|---|
| ORD ID | ord-9f0e81c85b0a4b208f11e51a5293d9ae |
|---|
| Source note | uspto-grants-2009_06 |
|---|
