HRID1986606

反应详情

EQUATION

反应方程式

HRID 1986606 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The process of preparing the compound of formula I comprises the steps of dissolving 3-isobutyl-1-methylxanthine (IBMX) into methanol and stirring with 2-bromoethylamine upon a mantle heater, reacting this mixture with NaOH and then recrystallizing this mixture with methanol to obtain N7-bromoehtyl 3-isobutyl-1-methylxanthine.

WORKUP

后处理

  1. customThe process of preparing the compound of formula I
  2. customrecrystallizing this mixture with methanol