HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 68908797, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Pentyl-8-azabicyclo[3.2.1]octane | HCID 21989852 | — |
| Product | HCID 68908797 | HCID 68908797 | — |
Reaction Steps
Crude (R,S)-1-(3-chloro-2-methylpropyl)-3,4-dihydro-1H-quinolin-2-one (107LH63) (0.094 g), 3-pentyl-8-azabicyclo[3.2.1]octane (0.027 g, 0.15 mmol), NaI (0.100 g, 0.67 mmol), and K2CO3 (0.075 g, 0.54 mmol) in DMF (1 mL) were reacted and purified according to GP20 to give the title compound (107LH74-c5) (0.023 g). HPLC-MS (ammonium acetate) [M+H]+=383.34.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07550459B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-fa7e939afde247bcad7839c438d6a8b1 |
| Source note | uspto-grants-2009_06 |