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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1986807Generated: October 29, 2026

Sodium Iodide → HCID 68908797, compound

https://huagongshe.com/reaction/1986807

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium IodideHCID 5238—
ReactantDimethylformamideHCID 6228—
ReactantPotassium CarbonateHCID 11430—
Reactant3-Pentyl-8-azabicyclo[3.2.1]octaneHCID 21989852—
ProductHCID 68908797HCID 68908797—

Reaction Steps

Crude (R,S)-1-(3-chloro-2-methylpropyl)-3,4-dihydro-1H-quinolin-2-one (107LH63) (0.094 g), 3-pentyl-8-azabicyclo[3.2.1]octane (0.027 g, 0.15 mmol), NaI (0.100 g, 0.67 mmol), and K2CO3 (0.075 g, 0.54 mmol) in DMF (1 mL) were reacted and purified according to GP20 to give the title compound (107LH74-c5) (0.023 g). HPLC-MS (ammonium acetate) [M+H]+=383.34.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07550459B2
Source datasetuspto-grants-2009_06
ORD IDord-fa7e939afde247bcad7839c438d6a8b1
Source noteuspto-grants-2009_06