Ammonium Acetate → HCID 55281960, compound

HRID 1986970Notes

Reaction equation

[CH2:1]([CH:3]1[CH2:8][C:7](=O)[CH2:6][C:5](=[O:10])[CH2:4]1)[CH3:2].C([O-])(=O)C.[NH4+:15]>>[NH2:15][C:7]1[CH2:8][CH:3]([CH2:1][CH3:2])[CH2:4][C:5](=[O:10])[CH:6]=1

Participants

Reactant 2

HCID 517165Ammonium Acetate

HCID 2734798HCID 2734798, compound

Product 1

HCID 55281960HCID 55281960, compound

Procedure

In close analogy to (Baraldi, P. G.; Simoni, D.; Manfredini, S.; Synthesis 1983, (11) 902-903) 5-ethylcyclohexane-1,3-dione was reacted with ammonium acetate to give the title compound.

Sources & evidence

ORD record: ord-45f4e105bfa741cba93fb4116109cd89
Source dataset: uspto-grants-2009_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07550482B2

Reaction notes

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