Hydrochloric Acid → HCID 69078521, compound

Participants

Reaction Steps

A solution of Boc-3-amino-2-methyl-4-phenylbutan-2-ol (0.34 g, 1.2 mmol) in 100 mL ethyl acetate was saturated with HCl gas and stirred at ambient temperature for 1 hour. The reaction was evaporated in vacuo to give 3-amino-2-methyl-4-phenylbutan-2-ol hydrochloride as a white solid: 1H NMR (400 MHz, CDCl3) δ 8.05 (bs, 2H), 7.33 (m, 5H), 3.34 (m, 1H), 3.02 (m, 2H), 1.37 (s, 3H), 1.33 (s, 3H).

Provenance & Evidence