Sodium Hydroxide → HCID 86605105, compound

Participants

Reaction Steps

Following a similar procedure to that described in example 2, but using N-[4-[4-chloro-5-(3-fluoro-4-methoxyphenyl)imidazol-1-yl]phenylsulfonyl]-phosphoramidic acid (obtained in example 6) instead of diethyl N-[4-[4-chloro-5-(3-fluoro-4-methoxyphenyl)imidazol-1-yl]phenylsulfonyl]phosphoramidate and 3 equivalents of NaOH instead of 1, and recrystallizing then the crude product obtained from PriOH, the title compound of the example was obtained as a white solid.

Provenance & Evidence