Acetylglycine → HCID 68819123, compound

Participants

Reaction Steps

20 g o-Trifluoromethyl benzaldehyde, 60 g N-acetylglycine and 12 g sodium acetate were stirred in 68.2 g acetic anhydride at 80° C. for 22 hrs. The mixture was poured into 100 ml ice water, the precipitate filtered off and washed with water. Yield 35 g of wet crude product, used without further purification fort the next step.

Provenance & Evidence