Allyl bromide → HCID 178456405, compound

HRID 1987508Notes

Reaction equation

HRID 1987508 reaction equation
[NH2:1][N:2]1[CH:6]=[CH:5][N:4]=[N:3]1.[CH2:7]([Br:10])[CH:8]=[CH2:9]>>[Br-:10].[NH2:1][N+:2]1[CH:6]=[CH:5][N:4]([CH2:9][CH:8]=[CH2:7])[N:3]=1

Participants

3

Reactant 2

HCID 7841Allyl bromideHCID 38257231H-1,2,3-triazol-1-amine

Product 1

HCID 178456405HCID 178456405, compoundYield 75%

Procedure

In the aforementioned method, 1-amino-1,2,3-triazole (2) 5.00 g (59.5 mmoles) was reacted with allyl bromide 35.00 g (289 mmoles) at 20° C., and upon work-up resulted in a yield of 9.03 g (75%) of 1-amino-3-(2-propenyl)-1,2,3-triazolium bromide (2d), mp 100-101° C.

Sources & evidence

ORD record
ord-78b29ebc09544a7b958fa682d7e221a4
Source dataset
uspto-grants-2009_06
Patent number
US07550601B1

Reaction notes

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