HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 178456405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 1H-1,2,3-triazol-1-amine | HCID 3825723 | — |
| Product | HCID 178456405 | HCID 178456405 | 75% |
Reaction Steps
In the aforementioned method, 1-amino-1,2,3-triazole (2) 5.00 g (59.5 mmoles) was reacted with allyl bromide 35.00 g (289 mmoles) at 20° C., and upon work-up resulted in a yield of 9.03 g (75%) of 1-amino-3-(2-propenyl)-1,2,3-triazolium bromide (2d), mp 100-101° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07550601B1 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-78b29ebc09544a7b958fa682d7e221a4 |
| Source note | uspto-grants-2009_06 |