Butyl bromide → HCID 178448583, compound

HRID 1987509Notes

Reaction equation

[NH2:1][N:2]1[CH:6]=[CH:5][N:4]=[N:3]1.[CH2:7]([Br:11])[CH2:8][CH2:9][CH3:10]>>[Br-:11].[NH2:1][N+:2]1[CH:6]=[CH:5][N:4]([CH2:7][CH2:8][CH2:9][CH3:10])[N:3]=1

Participants

Reactant 2

HCID 8002Butyl bromide

HCID 38257231H-1,2,3-triazol-1-amine

Product 1

HCID 178448583HCID 178448583, compound

Procedure

Using the same method as previously mentioned, 1-amino-1,2,3-triazole (2) 2.00 g (23.8 mmoles) was reacted with n-butyl bromide (16.01 g., 116.8 mmoles) at 60° C. Upon work-up, 4.12 g (78%) of 1-amino-3-butyl-1,2,3-triazolium bromide (2e) was recovered, mp 131-132° C.

Workup

customUpon work-up, 4.12 g (78%) of 1-amino-3-butyl-1,2,3-triazolium bromide (2e) was recovered

Sources & evidence

ORD record: ord-b7019816a14c48b7a900fe8da8c070a0
Source dataset: uspto-grants-2009_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07550601B1

Reaction notes

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