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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1987554생성일: 2026년 10월 26일

Benzyl 4-isobutyl-1-piperazinecarboxylate → 1-(2-Methylpropyl)piperazine

https://huagongshe.com/reaction/1987554

반응식

참여 물질

역할이름HCID투입량
반응물Benzyl 4-isobutyl-1-piperazinecarboxylateHCID 23069811—
촉매HCID 178418390HCID 178418390—
용매EthanolHCID 702—
생성물1-(2-Methylpropyl)piperazineHCID 2052052112.9%

반응 단계

The resulting benzyl 4-isobutylpiperazin-1-carboxylate (1.05 g) was dissolved in 35 mL of ethanol, 10% palladium-carbon (750 mg) was added thereto, and the reaction mixture was stirred at room temperature under hydrogen atmosphere (1 atm) for 12 hours. The palladium-carbon was removed by filtration, and the filtrate was evaporated to give the title compound (610 mg) as a colorless oil.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07550503B2
출처 데이터셋uspto-grants-2009_06
ORD IDord-ba36e911f4cd47d39b1bd4e218a2fe6f
출처 메모uspto-grants-2009_06