HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1987596Generated: November 1, 2026
2-Acetamido-5-aminopyridine → HCID 178466025, compound
https://huagongshe.com/reaction/1987596
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Acetamido-5-aminopyridine | HCID 2735219 | — |
| Reactant | HCID 178434119 | HCID 178434119 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178466025 | HCID 178466025 | — |
Reaction Steps
(Z)-4-(4-chloroquinolin-2(1H)-ylidene)-3-methyl-1H-pyrazol-5(4H)-one (0.033 g, 0.13 mmol) and 2-acetamido-5-aminopyridine (Matrix) (0.058 g, 0.38 mmol) were dissolved in ethanol (1.5 mL). The reaction mixture was heated to 180° C. using a microwave reactor for 6 hrs. The mixture was concentrated and purified by LC-MS to give the title compounds of Example 4 and Example 5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07550598B2 |
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| Source dataset | uspto-grants-2009_06 |
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| ORD ID | ord-d8d59679e9c241b99da44f5d531574ac |
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| Source note | uspto-grants-2009_06 |
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