HuagongsheHuagongshe Chemistry Print Report · For research reference only
Quinoline 1-oxide → HCID 178518890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Quinoline 1-oxide | HCID 15366 | — |
| Reactant | 5-Phenyl-4H-pyrazol-3-ol | HCID 78577 | — |
| Product | HCID 178518890 | HCID 178518890 | — |
Reaction Steps
The title compound was synthesized using 3-phenyl-1H-pyrazol-5(4H)-one and quinoline N-oxide according to the procedure described in Example 23. 1H NMR (400 MHz, DMSO-d6) 8 ppm 7.21 (d, J=9.09 Hz, 1H) 7.50-7.60 (m, 7H) 7.82 (t, J=7.71 Hz, 1H) 7.93 (t, J=6.82 Hz, 2H) 8.33 (d, J=8.84 Hz, 1H); ESI-MS: m/z calc'd for C18H13N3O 287.32. found 288.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07550598B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-1e1a41a0815c4fe8b16bf0221665cc0c |
| Source note | uspto-grants-2009_06 |